HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+)-1-(4-Nitrophenyl)-3-acetyl-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine → Gyki-53405
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+)-1-(4-Nitrophenyl)-3-acetyl-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine | HCID 9976222 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Gyki-53405 | HCID 126756 | — |
Reaction Steps
The title compound was prepared from the compound of Example 126 using the process described in Example 128. Melting point 169°-172° C. [α]D =-321.34° (c=1, MeOH) Enantiomeric purity: >99%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05519019 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-616fb46fb2d441f7a3d4b22a0ecf4205 |
| Source note | uspto-grants-1996_05 |