HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Pyridine-2,4-dicarboxylic acid dibenzyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 2,4-Pyridinedicarboxylic acid | HCID 10365 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Pyridine-2,4-dicarboxylic acid dibenzyl ester | HCID 14837626 | — |
Reaction Steps
30g of pyridine-2,4-dicarboxylic acid are converted into the acid chloride using 30 ml of thionyl chloride analogously to Example 1 and the acid chloride is reacted with 43.8 g of benzyl alcohol. The product is recrystallized from diisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05519038 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-4908211bbd3c400ab689a88f731cd432 |
| Source note | uspto-grants-1996_05 |