HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-(1-Naphthyl)cyclopropanecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-(1-Naphthyl)cyclopropanecarboxylic acid | HCID 12276450 | — |
| Product | 1-(1-Naphthyl)cyclopropanecarbonyl chloride | HCID 12276454 | — |
Reaction Steps
1-(1-Naphthyl)cyclopropane carboxylic acid (6.7 g, prepared in a similar manner to that described in Example H20), was added to thionyl chloride (25 ml) and the mixture heated at 90°-95° C. for 1 hour. Excess thionyl chloride was removed in vacuo to yield 1-(1-naphthyl)cyclopropanecarbonyl chloride (7.1 g) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05519034 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-9ac7747b1c1a4672a97ff7d019e61428 |
| Source note | uspto-grants-1996_05 |