HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[(4-Chlorophenyl)methylidene]-2,2-dimethylcyclopentan-1-one → 5-(4-Chlorobenzyl)-2,2-dimethylcyclopentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[(4-Chlorophenyl)methylidene]-2,2-dimethylcyclopentan-1-one | HCID 53421021 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(4-Chlorobenzyl)-2,2-dimethylcyclopentanone | HCID 11424896 | — |
Reaction Steps
5 g of 2-(4-chlorobenzylidene)-5,5-dimethylcylopentanone (prepared in Example 5) was dissolved in 40 ml of ethanol, and 60 mg palladium-carbon (10%) was added to the mixture. The hydrogenation reaction was carried out under normal pressure until theoretical amount of hydrogen was absorbed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05519160 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-374bf906581b40649dcba35c765543d2 |
| Source note | uspto-grants-1996_05 |