Sodium Hydroxide → HCID 22407394, compound

HRID 440582Notes

Reaction equation

HRID 440582 reaction equation
[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([O:17][CH:18]([C:25]([O:27]CC)=[O:26])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)=[CH:13][CH:12]=2)[C:8]2[CH:30]=[C:31]([N:34]3[CH2:39][CH2:38][CH2:37][NH:36][C:35]3=[O:40])[CH:32]=[CH:33][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4].[OH-].[Na+]>C(O)C>[CH2:1]([C:5]1[N:9]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([O:17][CH:18]([C:25]([OH:27])=[O:26])[C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=3)=[CH:13][CH:12]=2)[C:8]2[CH:30]=[C:31]([N:34]3[CH2:39][CH2:38][CH2:37][NH:36][C:35]3=[O:40])[CH:32]=[CH:33][C:7]=2[N:6]=1)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 22407534HCID 22407534, compound

Product 1

HCID 22407394HCID 22407394, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1b from 2-n-butyl-1-[4-[(α-ethoxycarbonyl)benzyloxy]benzyl]-6-(3,4,5,6-tetrahydro-2(1H)-pyrimidinon-1-yl)-benzimidazole and 1N sodium hydroxide solution in ethanol.

Sources & evidence

ORD record
ord-6505b987944248aaabfe887d7c82c356
Source dataset
uspto-grants-1996_05
Patent number
US05519138

Reaction notes

Loading…