HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphosgene → HCID 22404775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphosgene | HCID 10426 | — |
| Reactant | HCID 22404764 | HCID 22404764 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22404775 | HCID 22404775 | — |
Reaction Steps
By the method of Example 1, Step F, 2.51 g (0.011 mole) of 7-amino-4-chloro-2,3-dihydro-2,2-dimethylbenzofuran-3-thione is reacted with 2.18 g (0.011 mole) of trichloromethyl chloroformate in 65 mL of toluene, yielding 4-chloro-2,3-dihydro-2,2-dimethyl-3-thioxobenzofuran-7-yl isocyanate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521147 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-6c43d17c95204e62bb86374746308886 |
| Source note | uspto-grants-1996_05 |