HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 17879037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-(4-Methylphenoxy)benzoic acid | HCID 291994 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 17879037 | HCID 17879037 | — |
Reaction Steps
A solution of 2.0 g of 4-(4-methylphenoxy)benzoic acid in 30 ml of methylene chloride is added 1.67 g of oxalyl chloride and the mixture refluxed for 30 minutes with stirring under nitrogen. The reaction mixture is evaporated in vacuo to a residue which is evaporated with carbon tetrachloride(2×30 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521173 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-2f956dce5fef42dcab8db3a6eba15228 |
| Source note | uspto-grants-1996_05 |