Dimethylamine → HCID 178437451, compound

HRID 440858Notes

Reaction equation

[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]3[NH:25][N:24]=[N:23][N:22]=3)=[CH:11][CH:10]=2)[C:6]2[CH:26]=[C:27]([NH:31][C:32]3[C:35](=O)[C:34](=[O:37])[C:33]=3[O:38]CC)[CH:28]=[C:29]([CH3:30])[C:5]=2[N:4]=1)[CH3:2].[CH3:41][NH:42][CH3:43]>>[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]3[NH:25][N:24]=[N:23][N:22]=3)=[CH:11][CH:10]=2)[C:6]2[CH:26]=[C:27]([NH:31][C:32]3[C:33](=[O:38])[C:34](=[O:37])[C:35]=3[N:42]([CH3:43])[CH3:41])[CH:28]=[C:29]([CH3:30])[C:5]=2[N:4]=1)[CH3:2]

Participants

Reactant 2

HCID 674Dimethylamine

HCID 178467131HCID 178467131, compound

Product 1

HCID 178437451HCID 178437451, compound

Procedure

Prepared analogously to Example 14b from 4'-[[2-ethyl-4-methyl-6-[(2-ethoxy-3,4-dioxo-1-cyclobuten-1-yl)-amino]-1H -benzimidazol-1-yl]-methyl]-2-(1H-tetrazol-5-yl)biphenyl and dimethylamine.

Sources & evidence

ORD record: ord-99dd0da28e33440d99a366ec3a9fc822
Source dataset: uspto-grants-1996_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05521177

Reaction notes

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