Dimethylamine → HCID 178437459, compound

HRID 440860Notes

Reaction equation

[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]3[NH:25][N:24]=[N:23][N:22]=3)=[CH:11][CH:10]=2)[C:6]2[CH:26]=[C:27]([NH:31][C:32](=[N:41][S:42]([CH3:45])(=[O:44])=[O:43])OOC3C=CC=CC=3)[CH:28]=[C:29]([CH3:30])[C:5]=2[N:4]=1)[CH3:2].[CH3:46][NH:47][CH3:48]>>[CH2:1]([C:3]1[N:7]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[C:21]3[NH:22][N:23]=[N:24][N:25]=3)=[CH:11][CH:10]=2)[C:6]2[CH:26]=[C:27]([NH:31][C:32]([N:47]([CH3:48])[CH3:46])=[N:41][S:42]([CH3:45])(=[O:44])=[O:43])[CH:28]=[C:29]([CH3:30])[C:5]=2[N:4]=1)[CH3:2]

Participants

Reactant 2

HCID 674Dimethylamine

HCID 178437460HCID 178437460, compound

Product 1

HCID 178437459HCID 178437459, compound

Procedure

Prepared analogously to Example 14b from 4'-[[2-ethyl-4-methyl-6-(2-phenoxy-3-methylsulphonyl-isoureido)-1H-benzimidazol -1-yl]-methyl]-2-(1H-tetrazol-5-yl)-biphenyl and dimethylamine.

Sources & evidence

ORD record: ord-77069e7ebd3c4fe2991ef3618c927e61
Source dataset: uspto-grants-1996_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05521177

Reaction notes

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