HCID 583659, compound → HCID 22405788, compound

Participants

Reaction Steps

To a solution of 4.64 g of 4-[3-(2-pyridyl)-2-oxooxazolidin-5-yl]methoxynitrobenzene in 50 ml of 1,4-dioxane and 150 ml of N,N-dimethylformamide, 0.47 g of 10% palladium carbon was added, followed by stirring for 2.5 hours at room temperature and 5 atm. pressure under a hydrogen stream. The reaction mixture was filtered and the filtrate was then concentrated under reduced pressure. Methanol was added to the residue and the crystals so precipitated were collected by filtration, whereby 3.41 g of the title compound were obtained (yield: 81%).

Provenance & Evidence