HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetraethoxysilane → Benzene, 1,3-bis(1-phenylethenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetraethoxysilane | HCID 6517 | — |
| Reactant | Isoprene | HCID 6557 | — |
| Reactant | Pentamethyldiethylenetriamine | HCID 18196 | — |
| Reactant | 1,3-Diisopropenylbenzene | HCID 77353 | — |
| Reactant | CID 53628100 | HCID 178418400 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzene, 1,3-bis(1-phenylethenyl)- | HCID 118622 | — |
Reaction Steps
Isoprene, sec-BuLi solution (1.3 M in cyclohexane), anhydrous tetrahydrofuran (THF), pentamethyldiethylenetriamine (PMDETA), tetraethoxysilane, and 1,3-diisopropenylbenzene (1) were obtained from Aldrich Chemical Company, Milwaukee, Wis.. 1,3-bis(1-phenylethenyl)benzene (3) was obtained from the Dow Chemical Company, Midland, Mich.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521255 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-ee45394c1e9e4443b39dc261511611c5 |
| Source note | uspto-grants-1996_05 |