HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 18347198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 70215195 | HCID 70215195 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 18347198 | HCID 18347198 | 90.3% |
Reaction Steps
A solution of the product of Step 2 (100 mg), NBS (90 mg) and benzoyl peroxide in CCl4 (5 mL) was heated to reflux under a spotlight for 30 min. The mixture was cooled, diluted with Et2O (3 ml) and filtered. The filtrate was concentrated and the residue was purified by flash chromatography, eluted with 15:1 hexane/EtOAc to give the title compound (120 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521213 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-3a4dc85a5b264538926497be71faba93 |
| Source note | uspto-grants-1996_05 |