HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10347758, compound → HCID 10392960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10347758 | HCID 10347758 | — |
| Solvent | Dichloromethane ethylacetate | HCID 21226138 | — |
| Product | HCID 10392960 | HCID 10392960 | — |
Reaction Steps
Using a similar procedure to that described in Example 1, using ethyl acetate:dichloromethane (5:95) as the chromatography solvent, 2-(3-benzyloxycarbonylamino-2-oxo-6-phenethyl-1,2-dihydro-1-pyridyl)-N-(3,3,3-trifluoro-2-hydroxy-1-isopropylpropyl)acetamide was oxidized to afford the title product; HPLC: tR =6.16, FR=2.0, column A, water:acetonitrile (2:3); MS: m/z=558(M+1). Analysis for C29H30F3N3O5 :
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521179 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-415671150c9340d3923166841113b202 |
| Source note | uspto-grants-1996_05 |