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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 441174Generated: October 29, 2026

HCID 10347758, compound → HCID 10392960, compound

https://huagongshe.com/reaction/441174

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10347758HCID 10347758—
SolventDichloromethane ethylacetateHCID 21226138—
ProductHCID 10392960HCID 10392960—

Reaction Steps

Using a similar procedure to that described in Example 1, using ethyl acetate:dichloromethane (5:95) as the chromatography solvent, 2-(3-benzyloxycarbonylamino-2-oxo-6-phenethyl-1,2-dihydro-1-pyridyl)-N-(3,3,3-trifluoro-2-hydroxy-1-isopropylpropyl)acetamide was oxidized to afford the title product; HPLC: tR =6.16, FR=2.0, column A, water:acetonitrile (2:3); MS: m/z=558(M+1). Analysis for C29H30F3N3O5 :

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05521179
Source datasetuspto-grants-1996_05
ORD IDord-415671150c9340d3923166841113b202
Source noteuspto-grants-1996_05