HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 135623128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 1-(3-Hydroxynaphthalen-2-yl)-2-(methanesulfinyl)ethan-1-one | HCID 12715520 | — |
| Product | HCID 135623128 | HCID 135623128 | 55% |
Reaction Steps
A solution of 3'-hydroxy-2-(methylsulfinyl)-2'-acetonaphthone (10 g, 0.040 mole) in n-butylamine (50 ml) was stirred at room temperature for 24 hrs. The reaction mixture was poured into petroleum ether (400 ml) and the product, which precipitated, was filtered off. Recrystallization from absolute ethanol gave light brown crystals (7.0 g, 55%), mp 162°-164°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039579 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-3a91a647ba104c08a13b8c099a781f78 |
| Source note | uspto-grants-1977_08 |