HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acetate → Allyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acetate | HCID 6584 | — |
| Reactant | Methyl acetate methanol | HCID 11389366 | — |
| Product | Methanol | HCID 887 | 90% |
| Product | Allyl acetate | HCID 11584 | 92% |
Reaction Steps
The tandem tube reactors are operated as in Example 1, with substitution of 740 grams per hour of pure methyl acetate for the methyl acetate-methanol azeotrope. Analysis of the condensed phases indicates the collection per hour of 254 grams of methyl acetate (34% unconverted), 607 grams of allyl acetate (92% yield based on 66% conversion) and 191 grams of methanol (90% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039592 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-b5154e0c1d844b199d2917bb4dc8f405 |
| Source note | uspto-grants-1977_08 |