HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acetate → Methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acetate | HCID 6584 | — |
| Reactant | Methyl acetate methanol | HCID 11389366 | — |
| Product | Methanol | HCID 887 | 90% |
| Product | Allyl acetate | HCID 11584 | 89% |
Reaction Steps
The tandem tube reactors are operated as described in Example 2, with substitution of 740 grams per hour of pure methyl acetate for the methyl acetate-methanol azeotrope. Analysis of the condensed phases indicates the collection per hour of 157 grams of methyl acetate (21% unconverted), 705 grams of allyl acetate (89% yield based on 79% conversion), and 227 grams of methanol (90% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039592 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-efe053caa7ad478ba0f9f9348d4601d0 |
| Source note | uspto-grants-1977_08 |