HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluidine → HCID 21420822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | 1-Bromononane | HCID 12742 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21420822 | HCID 21420822 | — |
Reaction Steps
A stirred mixture of p-toluidine (1100 parts) and nonyl bromide (478 parts) was heated on a steam bath for 20 hours, cooled and diluted with water (200 parts). The mixture was then made alkaline with caustic soda and after separation of the aqueous phase the residual oil was distilled under reduced pressure to obtain N-nonyl-p-toluidine (452 parts) as a pale yellow oil boiling at 136°-140° C. at 0.8 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039612 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-d789c5bc99254f0d8e4f1e3a21c9aa73 |
| Source note | uspto-grants-1977_08 |