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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 441363Generated: November 2, 2026

p-Toluidine → HCID 21420822, compound

https://huagongshe.com/reaction/441363

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-ToluidineHCID 7813—
Reactant1-BromononaneHCID 12742—
ReactantSodium HydroxideHCID 14798—
SolventWaterHCID 962—
ProductHCID 21420822HCID 21420822—

Reaction Steps

A stirred mixture of p-toluidine (1100 parts) and nonyl bromide (478 parts) was heated on a steam bath for 20 hours, cooled and diluted with water (200 parts). The mixture was then made alkaline with caustic soda and after separation of the aqueous phase the residual oil was distilled under reduced pressure to obtain N-nonyl-p-toluidine (452 parts) as a pale yellow oil boiling at 136°-140° C. at 0.8 mm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04039612
Source datasetuspto-grants-1977_08
ORD IDord-d789c5bc99254f0d8e4f1e3a21c9aa73
Source noteuspto-grants-1977_08