HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21421165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Hydroxyisobutyric acid | HCID 11671 | — |
| Reactant | 4-(phenoxymethyl)phenol | HCID 316177 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21421165 | HCID 21421165 | — |
Reaction Steps
A mixture of 20 g. of 4-phenoxymethylphenol and 13.2 g. of the ethyl ester of 2-hydroxyisobutyric acid is combined with 15 g. of sulfuric acid, and the reaction mixture is agitated for 2 hours at 50°-60°. After cooling, the mixture is combined with water and worked up as usual, obtaining the ethyl ester of 2-(4-phenoxymethylphenoxy)-2-methyl-propionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039683 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-f2df38affc454978b39c2052958752ee |
| Source note | uspto-grants-1977_08 |