Diallylamine → HCID 21419179, compound

Participants

Reaction Steps

A solution of 2.6 g. of 88 percent 1-methyl-1,2,4,5-tetrahydro-3,2-benzoxazepine-2-carbonyl chloride in 20 ml. of dichloromethane was added at room temperature to a solution of 2.23 g. of diallylamine in 30 ml. of dichloromethane. The mixture was then refluxed for two hours and after cooling was washed sequentially with aqueous 5 percent HCl, with aqueous sodium bicarbonate and with water. The organic layer was dried over Na2SO4 and evaporated to dryness. The residue was distilled at 140° C./0.02 mm Hg. Yield 2.3 g.

Provenance & Evidence