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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 441511Generated: October 26, 2026

Sodium Hydroxide → Diazene, (nitrophenyl)phenyl-, (E)-

https://huagongshe.com/reaction/441511

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
Reactant2-Nitro-2'-hydroxy-3',5'-bis(tert-amyl)azobenzeneHCID 104111—
ProductDiazene, (nitrophenyl)phenyl-, (E)-HCID 142206—

Reaction Steps

The same procedure as described in Example 1 was carried out except that the 27.4 grams of 50% sodium hydroxide was used with 155 grams of 2'-hydroxy-3',5'-di-tert-amyl-2-nitroazobenzene to give a ratio of moles of alkali to moles of o-nitroazobenzene intermediate of 0.848/1 compared to the ratio of 0.42/1 employed in Example 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04041044
Source datasetuspto-grants-1977_08
ORD IDord-2d3d8654b82045978a53888e521b7675
Source noteuspto-grants-1977_08