HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 12230454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Tryptophol | HCID 10685 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12230454 | HCID 12230454 | — |
Reaction Steps
A solution of tryptophol (8 g, 0.05M), acetone (5 g) and p-toluenesulfonic acid (100 mg) in 100 ml benzene containing hydrated alkali-aluminum silicate (Molecular Sieves No. 4) is heated to reflux for 1 hr. More p-toluenesulfonic acid (100 mg) and the ketone, acetone (3 g), is added and the reflux contained for a further 1.5 hr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04041169 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-6755dbaba82848aeb24e2bbea8fa9082 |
| Source note | uspto-grants-1977_08 |