Ethanol → HCID 70632723, compound

HRID 441705Notes

Reaction equation

HRID 441705 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:11]([OH:13])=[O:12])[CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:14]([OH:16])=[O:15].[NH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH2:24].C(O)C>O>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:11]([O-:13])=[O:12])[CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:14]([O-:16])=[O:15].[NH3+:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][NH3+:24]

Participants

5

Reactant 3

HCID 702EthanolHCID 16402HexamethylenediamineHCID 117905982,7-Naphthalenedicarboxylic acid

Product 1

HCID 70632723HCID 70632723, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Equimolar proportions of naphthalene-2,7-dicarboxylic acid and hexamethylene diamine were dissolved in water to form a salt. Then, ethyl alcohol was added to form hexamethylene diammonium naphthalene-2,7-dicarboxylate as a white powder which did not contain water of crystallization.

Workup

  1. customto form a salt

Sources & evidence

ORD record
ord-89b3ed993bcc4e06bae1601768fba416
Source dataset
uspto-grants-1977_08
Patent number
US04042571

Reaction notes

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