HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Cresol → 1-Methyl-4-[(3-methylbut-2-en-1-yl)oxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Cresol | HCID 2879 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Methyl-4-[(3-methylbut-2-en-1-yl)oxy]benzene | HCID 13328333 | — |
Reaction Steps
A mixture of p-cresol and sodium hydroxide was stirred with dimethylformamide and water while 1-bromo-3-methylbut-2-ene (VII; R1 = R2 = CH3, Hal = Br) was added dropwise. The 1-(p-methylphenoxy-3-methylbut-2-ene was isolated as described under Example B(i).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04042589 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-0a4412b1c7fd479390d2e3225893fe8d |
| Source note | uspto-grants-1977_08 |