HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → Formamide, N,N-dioctyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | N-Methyl-N-octyl-1-octanamine | HCID 78202 | — |
| Product | Formamide, N,N-dioctyl- | HCID 221420 | 4.5% |
Reaction Steps
By essentially the procedure of Example 1, a tube was charged with 40 g of methyldioctylamine and 1.0 g of CuCl2. 2H2O. The reaction was run at 109°-120° C. for 25 min while oxygen (0.2 mole) was injected incrementally at 160-275 psi. GC/MS analysis showed a 72.0% conversion of methyldioctylamine and a 4.5% yield of dioctylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04042621 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-77361349d68144e39a3db9d888a8dfa9 |
| Source note | uspto-grants-1977_08 |