Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxygen → Diphenylformamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxygen | HCID 977 | — |
| 반응물 | Methyldiphenylamine | HCID 11098 | — |
| 생성물 | Diphenylformamide | HCID 69081 | 43.3% |
반응 단계
By essentially the procedure of Example 1, a tube was charged with 40 g of methyldiphenylamine and 2.0 g CuCl2. 2H2O. The reaction was run at 115°-125° C. for 2 hr at 290-400 psi. About 0.1 mole of oxygen was injected incrementally. GC/MS analysis showed a 98.6% conversion of methyldiphenylamine and a 43.3% yield of diphenylformamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04042621 |
| 출처 데이터셋 | uspto-grants-1977_08 |
| ORD ID | ord-9030a9fdf81e4b68b1daa6a663d70bb7 |
| 출처 메모 | uspto-grants-1977_08 |