HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 66911312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 7-fluoro-3,4,4a,8a-tetrahydro-1H-quinolin-2-one | HCID 66911309 | — |
| Product | HCID 66911312 | HCID 66911312 | — |
Reaction Steps
This intermediate was obtained according to general procedure I from 7-fluoro-3,4,4a,8a-tetrahydro-1H-quinolin-2-one (92 mg, 0.56 mmol) and NBS (104 mg, 0.58 mmol) after flash chromatography on silica gel (hexanes/ethyl acetate, 5/1, Rf=0.27) as white solid (120 mg, 0.49 mmol, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541404B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-52795b1d40a3445db87ae26b7420f72b |
| Source note | uspto-grants-2013_09 |