HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furanol, tetrahydro- → HCID 21418205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furanol, tetrahydro- | HCID 9960 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | p-Toluenesulfonate | HCID 85570 | — |
| Reactant | HCID 21418186 | HCID 21418186 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21418205 | HCID 21418205 | — |
Reaction Steps
6-Hydroxy-2-methylisoquinolinium bromide (2.4 g.), sodium carbonate (5 g.) and 3-hydroxytetrahydrofuran, p-toluenesulphonate (5 g.) in acetonitrile (100 ml) were heated under reflux for 60 hours. The mixture was cooled and diluted with ether. The solid that crystallised was collected and had m.p. 144°-146°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04042697 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-cb8bfa525e00411c89bda71313c4331c |
| Source note | uspto-grants-1977_08 |