HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13050190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N,N'-[1-(4-Nitrophenyl)ethane-1,2-diyl]diacetamide | HCID 13050187 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13050190 | HCID 13050190 | — |
Reaction Steps
A solution of 4 g (0.015 mol) of N,N'-Diacetyl-1-(p-Nitrophenyl)-ethylenediamine in a mixture of 20 ml glacial acetic acid and 30 ml conc. HCl was heated at reflux for 24 hr and then cooled in ice. Upon filtration, 2.5 g (66%) of the crystalline 1-(p-Nitrophenyl)-ethylenediamine Dihydrochloride was collected. Anal. (C8H13N3O2Cl2) C, H, N were within 0.4% of theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04043998 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-8d26c6cf5bee43028fa812402c08dd74 |
| Source note | uspto-grants-1977_08 |