HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4-Diethoxy-2-methylbut-2-enal → 2-Methyl-4,4-diethoxybutanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4-Diethoxy-2-methylbut-2-enal | HCID 53905803 | — |
| Reactant | 4-Bromo-2-methylbut-2-enal | HCID 54511822 | — |
| Product | 2-Methyl-4,4-diethoxybutanal | HCID 21416341 | 89% |
Reaction Steps
The procedure described in Example 3 is repeated but 11.9 g of 2-methyl-4,4-diethoxy-2-butenal is used insteat of 16.3 g of 2-methyl- 4-bromo-2-butenal. Pure 2-methyl-4,4-diethoxybutanal is obtained in a yield of 89% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044026 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-f617526e1dfa476ab1e32487ae30f8f8 |
| Source note | uspto-grants-1977_08 |