Methyl iodide → HCID 86735016, compound
Reaction equation
[N+:1]([C:4](=[C:13]1[NH:18][CH2:17][CH2:16][CH2:15][S:14]1)[C:5]([O:7][CH:8]([CH3:12])[CH2:9][S:10][CH3:11])=[O:6])([O-:3])=[O:2].[CH3:19][I:20]>>[I-:20].[CH3:11][S+:10]([CH3:19])[CH2:9][CH:8]([O:7][C:5](=[O:6])[C:4]([N+:1]([O-:3])=[O:2])=[C:13]1[NH:18][CH2:17][CH2:16][CH2:15][S:14]1)[CH3:12]Participants
3
Procedure
9 was prepared as a yellow solid, m.p.: 113°-114°, by treating 9A with methyl iodide according to the procedure described in Example 1. EXAMPLE 10
Workup
- custom9 was prepared as a yellow solid, m.p.: 113°-114°
Sources & evidence
- ORD record
- ord-7f5ce0889fe54cb38d8abcf07c073444
- Source dataset
- uspto-grants-1977_08
- Patent number
- US04044128
Reaction notes
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