HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 20340702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Benzene, 1,1'-(1,3-propanediylbis(oxy))bis- | HCID 136562 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 20340702 | HCID 20340702 | — |
Reaction Steps
1,3-Diphenoxypropane (22.8 g), benzoyl chloride (31 g) and anhydrous aluminum chloride (33 g) are reacted in 1,2-dichloroethane (300 ml) for eighteen hours at 70° to yield 33.4 g (77% of theory) of colorless crystals mp 146°-148°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044139 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-8062cd0d87304406a140ae37bfea4ae1 |
| Source note | uspto-grants-1977_08 |