HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → o-Bromomethylphenylacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | [2-(Bromomethyl)phenyl]acetic acid | HCID 12889260 | — |
| Product | o-Bromomethylphenylacetyl chloride | HCID 12211419 | — |
Reaction Steps
A solution of 0.18 g of o-bromomethylphenylacetic acid in excess thionyl chloride is stirred at room temperature for 18 hours after which the unreacted thionyl chloride is removed under high vacuum to give o-bromomethylphenylacetyl chloride as an oily residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045438 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-6afef0337a3b44f9a0deeb7a168eb7cd |
| Source note | uspto-grants-1977_08 |