HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-2-nitrobenzoic acid → 5-Methyl-2-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-2-nitrobenzoic acid | HCID 18371 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 5-Methyl-2-nitrobenzoyl chloride | HCID 3016013 | — |
Reaction Steps
A mixture of 5-methyl-2-nitrobenzoic acid (3.6 g, 19.87 mmol) and thionyl chloride (18 mL) was stirred under reflux for 20 hours then concentrated under reduced pressure to give 5-methyl-2-nitrobenzoyl chloride (3.77 g) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541407B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-2380136c791e4cb694bce3db9ce279d8 |
| Source note | uspto-grants-2013_09 |