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HRID442494

反应详情

EQUATION

反应方程式

HRID 442494 的结构方程式

REACTANTS

反应物

2
结构：CC(C)NC(C)C
HCID7912

Diisopropylamine

C6H15N

结构：CCCc1ncc(C(=O)O)s1
HCID65773

Tizoprolic acid

C7H9NO2S

PRODUCTS

生成物

1
结构：CC(C)[NH2+]C(C)C.CCCc1ncc(C(=O)[O-])s1
HCID21415066

未命名化合物

收率 90%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

4.45 Grams of 2-propyl-5-thiazolecarboxylic acid (obtained in Example II) are dissolved in 120 cc of acetone and 2.62 gm of diisopropylamine are added. The solvent is evaporated off under low pressure and the crystals thus obtained are recrystallized from isopropyl ether. The diisopropylammonium 2-propyl-5-thiazolecarboxylate is obtained in the form of colorless crystals, soluble in water and in alcohol, melting at 120° C. (Yield: 90%).

WORKUP

后处理

  1. customThe solvent is evaporated off under low pressure
  2. customthe crystals thus obtained
  3. customare recrystallized from isopropyl ether