HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Ethanedithiol → 9-(Prop-2-en-1-yl)-9,10-dihydro-9,10-ethanoanthracene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Ethanedithiol | HCID 33645 | — |
| Reactant | HCID 68119883 | HCID 68119883 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | 9-(Prop-2-en-1-yl)-9,10-dihydro-9,10-ethanoanthracene | HCID 54033539 | — |
Reaction Steps
9-β-Propenyl-9,10-dihydro-9,10-ethanoanthracene (xi) is prepared from 9-β-propenyl-9,10-dihydro-9,10-ethanoanthracen-11-one (x) by a Wolff-Kishner reduction or treatment with ethanedithiol and then with hydrogen in the presence of Raney nickel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045560 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-0054e8fcbcd34c85abc0397a07ae1b93 |
| Source note | uspto-grants-1977_08 |