HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(9,10-Methanoanthracen-9(10H)-yl)prop-2-enoic acid → HCID 12507124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(9,10-Methanoanthracen-9(10H)-yl)prop-2-enoic acid | HCID 54454291 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12507124 | HCID 12507124 | — |
Reaction Steps
A mixture of β-(9,10-dihydro-9,10-methano-9-anthryl)acrylic acid (612 mg) and 5% palladium-charcoal (120 mg) in ethanol was stirred under hydrogen atmosphere at room temperature for 2 hours. The catalyst was removed by filtration, and the solution was evaporated to dryness to give β-(9,10-dihydro-9,10-methano-9-anthryl)propionic acid, M.P. 185° - 189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045560 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-a7e3b4f3c10247978b5e465c9ba5b1b2 |
| Source note | uspto-grants-1977_08 |