HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Chloride → HCID 70590206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Chloride | HCID 5284359 | — |
| Reactant | Sodium (2-amino-3-benzoylphenyl)acetate--water (1/1/1) | HCID 23663941 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70590206 | HCID 70590206 | — |
Reaction Steps
A stirred solution of 5 g. of sodium 2-amino-3-benzoylphenylacetate hydrate (0.02 mole) in 50 ml. of water was treated with 1.2 g. of calcium chloride (0.01 mole) in 10 ml. of water. An immediate precipitate developed. After an additional 15 min. stirring the precipitate was collected. Recrystallization from ethanol-water gave bright yellow needles which melted over the broad range of 160°-240° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045576 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-1b89d2a281fc4a18bcd69ed2409da59e |
| Source note | uspto-grants-1977_08 |