Silver Nitrate → Silver behenate

HRID 442605Notes

Reaction equation

HRID 442605 reaction equation
[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Na+].[N+]([O-])([O-])=O.[Ag+:30]>O>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Ag+:30]

Participants

4

Reactant 2

HCID 24470Silver Nitrate2×HCID 23668838Sodium Behenate2×

Product 1

HCID 164971Silver behenate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A silver behenate dispersion was prepared as described for INVENTION EXAMPLE 1, except that the dispersing medium used was a solution of 62 g gelatin (type 7598 from AGFA GELATINFABRIK vorm. KOEPFF & SOEHNE) in 1 L of distilled water instead of 30 g gelatin in 750 mL of distilled water; the addition rate of the sodium behenate solution was 8.3 mL/min instead of 46.6 mL/min; and the silver nitrate solution concentration was 0.246M instead of 2.94M. 0.092 moles of sodium behenate and 0.123 moles of silver nitrate were utilized in the reaction.

Sources & evidence

ORD record
ord-69fa3a4d44ef4b0ea19ea134089627f0
Source dataset
uspto-grants-1999_04
Patent number
US05891616

Reaction notes

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