HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarboxaldehyde → HCID 18788450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarboxaldehyde | HCID 10371 | — |
| Reactant | HCID 22323652 | HCID 22323652 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18788450 | HCID 18788450 | — |
Reaction Steps
2.92 g of 3-pyridyl carboxaldehyde are added to a solution of 4.82 g of N-(tert.butoxycarbonyl)ethanediamine in 50 ml of toluene in the presence of a dehydrating agent (4 Å molecular sieves) at about 5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05891894 |
| Source dataset | uspto-grants-1999_04 |
| ORD ID | ord-41f928836f4542bc8668c5e3653d0563 |
| Source note | uspto-grants-1999_04 |