HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 54224549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | ethyl 2-(4-bromobenzoyl)-2-(9H-xanthen-9-yl)acetate | HCID 54346958 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54224549 | HCID 54224549 | — |
Reaction Steps
Ethyl 2-(4-bromobenzoyl)-2-(9H-xanthen-9-yl)acetate (10.0 g, 0.02 mol) was heated in a solution of dimethylsulphoxide (100 ml) and water (0.72 ml) following the procedure described in Example (iv) to give 1-(4-bromophenyl)-2-(9H-xanthen-9-yl)ethanone as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05891899 |
| Source dataset | uspto-grants-1999_04 |
| ORD ID | ord-ce0b86daa8354f99b612122942ab3811 |
| Source note | uspto-grants-1999_04 |