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HRID4429

反应详情

EQUATION

反应方程式

HRID 4429 的结构方程式

REACTANTS

反应物

2
结构：CN(C)c1ccccc1
HCID949

N,N-Dimethylaniline

C8H11N

结构：CC(Cl)OC(=O)Oc1cccc2c1OC(C)(C)C2
HCID13557095

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)Oc1cccc2c1OC(C)(C)C2
HCID2566

Carbofuran

C12H15NO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

The procedure is as in (a) followed by (b), but pyridine is replaced by N,N-dimethylaniline and the intermediate carbonate is not distilled. Starting with 16.4 g of 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 16.8 g (76%) of CARBOFURAN are then obtained, M.p. 147° C.

WORKUP

后处理

  1. distillationthe intermediate carbonate is not distilled
  2. customare then obtained