HCID 53912156, compound → HCID 54474084, compound

Participants

Reaction Steps

To an ethanol solution (6.3 ml) of ethyl 8,8,8-triphenyloct-5-enoate (626 mg) was added 10% Pd-C (188 mg). The mixture was subjected to catalytic hydrogenation for six hours at ambient temperatures under atmospheric pressure. The catalyst was filtered off and the filtrate was concentrated under reduced pressure. The concentrate was purified by means of a silica gel column chromatography (hexane:ethyl acetate=10:1) to afford 620 mg of the title compound.

Provenance & Evidence