HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isocyanate → N-(3-Cyanothiophen-2-ylcarbamoyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isocyanate | HCID 78210 | — |
| Reactant | 2-Aminothiophene-3-carbonitrile | HCID 736607 | — |
| Product | N-(3-Cyanothiophen-2-ylcarbamoyl)benzamide | HCID 57456909 | — |
Reaction Steps
Prepared as in Example 1a from 2-aminothiophene-3-carbonitrile and benzoyl isocyanate as a white solid. 1H NMR (400 MHz, DMSO-d6) δ7.23-7.19 (m, 2H), 7.55 (t, J=8.0 Hz, 2H), 7.70-7.66 (m, 1H), 8.04-8.02 (m, 2H), 11.62 (bs, 1H), 12.18 (bs, 1H). MS 272 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541421B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-aaa32e6826d44096a93eb47d72bc88d2 |
| Source note | uspto-grants-2013_09 |