Methoxyacetyl chloride → HCID 12726865, compound

HRID 443498Notes

Reaction equation

HRID 443498 reaction equation
[NH:1]([C:3]1[N:4]=[N:5][C:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:7][CH:8]=1)[NH2:2].[CH3:15][O:16][CH2:17][C:18](Cl)=O>O1CCOCC1>[CH3:15][O:16][CH2:17][C:18]1[N:4]2[N:5]=[C:6]([C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=3)[CH:7]=[CH:8][C:3]2=[N:1][N:2]=1

Participants

4

Reactant 2

HCID 96623Methoxyacetyl chlorideHCID 64098423-Hydrazinyl-6-phenylpyridazine

Product 1

HCID 12726865HCID 12726865, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

To a mixture of 0.01 mole of 3-hydrazino-6-phenylpyridazine in 25 ml. of dioxane is added 0.005 mole of methoxyacetyl chloride. The mixture is refluxed for 2 hours to give the product of the Example, m.p. 133° C.

Workup

  1. temperatureThe mixture is refluxed for 2 hours
  2. customto give the product of the Example, m.p. 133° C.

Sources & evidence

ORD record
ord-f6b7e9a475ec4ea2810c160e26b992d1
Source dataset
uspto-grants-1981_04
Patent number
US04260755

Reaction notes

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