4-Methylthiobenzoyl chloride → HCID 53748532, compound

HRID 443587Notes

Reaction equation

HRID 443587 reaction equation
[C:1]([C:4]1[NH:5][CH:6]=[NH+:7][C:8]=1[O-:9])(=[O:3])[NH2:2].[CH3:10][C:11]1[CH:19]=[CH:18][C:14]([C:15](Cl)=[S:16])=[CH:13][CH:12]=1>>[CH3:10][C:11]1[CH:19]=[CH:18][C:14]([C:15]([O:9][C:8]2[N:7]=[CH:6][NH:5][C:4]=2[C:1](=[O:3])[NH2:2])=[S:16])=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 155550054-Methylthiobenzoyl chlorideHCID 178513830HCID 178513830, compound

Product 1

HCID 53748532HCID 53748532, compoundYield 96.2%

Procedure

1.258 g of 5-carbamoyl-1H-imidazol-4-yl p-methylthiobenzoate was synthesized from 0.636 g of 4-carbamoylimidazolium-5 olate and 1.4 g of p-methylthiobenzoyl chloride.

Sources & evidence

ORD record
ord-0f539668bd40483d9301e2b359e76d2e
Source dataset
uspto-grants-1981_04
Patent number
US04260774

Reaction notes

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