HRID443635
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 14.4 g. of 2-naphthol, 12.1 g. of 2-bromoethanol and 5.9 g. of sodium methoxide in 100 ml. of ethanol is allowed to stand two days at room temperature. The solvent is removed under vacuum and the residue extracted with ether. The ether extract is washed with water, dried (magnesium sulfate) and the solvent removed under vacuum to give crystals, m.p. 65°-70° C.
WORKUP
后处理
- customThe solvent is removed under vacuum
- extractionthe residue extracted with ether
- extractionThe ether extract
- washis washed with water
- dry with materialdried (magnesium sulfate)
- customthe solvent removed under vacuum
- customto give crystals, m.p. 65°-70° C.