Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane → 2-(2-Naphthyloxy)ethyl methanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | 2-(2-Naphthoxy)ethanol | HCID 7131 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 2-(2-Naphthyloxy)ethyl methanesulfonate | HCID 19004383 | — |
반응 단계
As described in Example 2, 13.5 g. of 2-(2-naphthyloxy)ethanol in 400 ml. of dichloromethane is reacted with 9.5 g. of methanesulfonyl chloride in the presence of 11.4 g. of triethylamine to give the product as tan crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04260816 |
| 출처 데이터셋 | uspto-grants-1981_04 |
| ORD ID | ord-e0de3a90955d439684568c996684aa72 |
| 출처 메모 | uspto-grants-1981_04 |