HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23468282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 23468285 | HCID 23468285 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23468282 | HCID 23468282 | — |
Reaction Steps
A solution of 3.2 g. of methyl 3-[2-(1-naphthyloxy)ethylamino]benzoate and 1.68 g. of potassium hydroxide in 40 ml. of 95% ethanol is heated to reflux for 4 hours. After cooling and diluting with 80 ml. of water, the solution is acidified with concentrated HCl and filtered. Recrystallization from acetonitrile affords the white desired product, m.p. 150°-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04260816 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-17cf8ff52432430b9e89a11628ee7de7 |
| Source note | uspto-grants-1981_04 |