Sodium Methoxide → HCID 23714401, compound

HRID 443650Notes

Reaction equation

HRID 443650 reaction equation
C[O-].[Na+:3].[C:4]1([O:14][CH2:15][CH2:16][NH:17][C:18]2[CH:26]=[CH:25][C:21]([C:22]([OH:24])=[O:23])=[CH:20][CH:19]=2)[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH:7]=[CH:6][CH:5]=1>CO>[C:4]1([O:14][CH2:15][CH2:16][NH:17][C:18]2[CH:19]=[CH:20][C:21]([C:22]([O-:24])=[O:23])=[CH:25][CH:26]=2)[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH:7]=[CH:6][CH:5]=1.[Na+:3]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 23468289HCID 23468289, compound

Product 1

HCID 23714401HCID 23714401, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of 1.42 g. sodium methoxide in 250 ml. methanol is added 8.0 g. of 4-[2-(1-naphthyloxy)ethylamino]benzoic acid. After one-half hour, the mixture is concentrated under vacuum to a solid which is washed with methanol and then CH2Cl2. This solid is immediately dried in a vacuum oven to minimize absorption of moisture from the air.

Workup

  1. waitAfter one-half hour
  2. concentrationthe mixture is concentrated under vacuum to a solid which
  3. washis washed with methanol
  4. customThis solid is immediately dried in a vacuum oven
  5. customabsorption of moisture from the air

Sources & evidence

ORD record
ord-1966e11a73dd46e59f649f2cabd145f9
Source dataset
uspto-grants-1981_04
Patent number
US04260816

Reaction notes

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