HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → 2-(4-Acetoxy-trans-2-butenyloxy)-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-(4-Chloro-trans-2-butenyloxy)-benzaldehyde | HCID 15572710 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-(4-Acetoxy-trans-2-butenyloxy)-benzaldehyde | HCID 20555652 | — |
Reaction Steps
The mixture of 50 g of 2-(4-chloro-trans-2-butenyloxy)-benzaldehyde, 50 g of sodium acetate and 200 ml of acetic acid is refluxed for 2 hours and concentrated. The concentrate is diluted with water, extracted with diethyl ether, the extract washed with water and 5% aqueous sodium bicarbonate, dried and evaporated, to yield the 2-(4-acetoxy-trans-2-butenyloxy)-benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04261907 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-7aee70f6ed20466fb2c8d0c4dad1736a |
| Source note | uspto-grants-1981_04 |